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Lunar Soil Analysis

NEW MEASUREMENTS OF THE PARTICLE SIZE DISTRIBUTION OF APOLLO 11 LUNAR SOIL

Introduction
NASA initiated a major new program to determine the grain size distribution of nearly all lunar soils collected in the Apollo program. Nearly all of these studies were done by sieving the samples, usually with a working fluid such as Freon™ or water. NASA measured the particle size distribution of lunar soil 10084,2005 in water, using a Microtrac™ laser diffraction instrument. Details of their sieving technique and protocol are given in the published report.  While sieving usually produces accurate and reproducible results, it has disadvantages.
Conclusion
Direct comparison of sieve data to lightscattering data is difficult and the results must be carefully checked with standard known particle sizes and distribution. NASA analyses of NIST or NISTtraceable grain size material shows that the Microtrac results are within acceptable ranges for particle sizes between 0.33μm and ~60μm. The correspondence of the sieve data from 10084 to the light-scattering data is good and provides confidence that the two methods produce comparable results. These results open the door to future automated, rapid, and reproducible grain size analysis of planetary soils and dust. ©2009 Lunar and Planetary Science Conference

D. S. McKay (NASA Johnson Space Center), B. L. Cooper, and L. M. Riofrio (Oceaneering Space Systems)

 

Sintering of Lunar and Simulant Glass

Abstract
Most oxygen-extraction techniques are temperature-dependent, with higher temperatures resulting in higher oxygen yield. An example is hydrogen reduction, in which the optimum process temperature is 1050°C. However, glass-rich lunar soil begins to show the effects of sintering at temperatures of 900°C or lower. Sintering welds particles together due to viscous relaxation of the glass in the sample. One approach to avoid problems related to sintering, such as difficulty in removing waste material from the reactor, is to keep the soil in motion. One of several methods being studied to accomplish this is fluidized-bed processing techniques, in which the grains are kept in motion by the action of flowing reductant gas. The spent material can be removed from the chamber while still fluidized, or the fluidizing motion can continue until the material has cooled below ~500°C. Until end-to-end prototypes are built that can remove the heated soil, the most practical option is to keep the bed fluidized while cooling the waste material.
As ISRU technology advances, another option will become valuable, which is to intentionally sinter the material to a great enough extent that it becomes a brick. The free iron in lunar soil is magnetic, and ferromagnetic bricks can be manipulated by robotic systems using electromagnetic end effectors. Finally, if an electromagnetic field is applied to the soil while the brick is being formed, the brick itself will become a magnet. This property can be used to create self-aligning bricks or other building materials that do not require fasteners. Although sintering creates a challenge for early lunar surface systems, knowledge gained during prototype development will be valuable for the advanced lunar outpost. ©2007 NASA
Keywords: hydrogen reduction, fluidized bed, fluidizing, channeling, sintering, oxygen production, lunar surface systems

Bonnie L. Cooper, Robotics and Automation Group, Oceaneering Space Systems, Houston TX 77058

 

Grinding Crystalline Silica

ENHANCED CHEMICAL REACTIVITY OF CRYSTALLINE QUARTZ BY MECHANICAL GRINDING

Summary: NASA has developed a technique for mechanically grinding crystalline silica which increases the chemical reactivity of the material as judged by the terephthalate assay. This technique uses a modern, commercially available ball mill. It provides a method for generating “fresh fractured” or “activated” silica to serve as a positive control for studies of lunar regolith chemical reactivity. The technique generates sufficient quantities of activated material (250 mg – 750 mg) to provide a ready source for biological and chemical studies. The technique may serve as a valuable method for applications with lunar regolith and other planetary materials which exhibit activation when mechanically ground.  ©2009 Lunar and Planetary Science Conference

E. Tranfield, J. C. Rask, W.T. Wallace, R. Kerschmann, D. J. Loftus.
Space Biosciences Division, NASA Ames Research Center
Habitability and Environmental Factors Division, NASA Lyndon B. Johnson Space Center

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